RIS ID

116309

Publication Details

Yu, L., Li, Y., Wang, X., Wang, X., Zhou, P., Jiang, S. & Pan, X. (2017). Consecutive reduction, radical-cyclization, and oxidative-dehydrogenation reaction of ortho-substituted diboryl compounds. Chemical Communications, 53 (70), 9737-9740.

Abstract

An elegant synthetic route to a ladder-type di-borate compound 2a was reported based on the reduction, radical-cyclization, and oxidative-dehydrogenation reaction of 1. The existence of the biradical intermediate [1●●]2- was supported by both EPR measurements and DFT calculations.

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Link to publisher version (DOI)

http://dx.doi.org/10.1039/c7cc05689c